Advanced Nanomaterials, Two Volume Edition by Kurt E. Geckeler, Hiroyuki Nishide

By Kurt E. Geckeler, Hiroyuki Nishide

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Extra info for Advanced Nanomaterials, Two Volume Edition

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These types of initiator contain a thermally cleavable C–O bond attached to a nitroxyl radical species. 2). An advantage to SFRP is that the chemical rate of this detachment drops almost to zero at room temperature. 2 The general mechanism of stable free radical polymerizations. 11 12 1 Phase-Selective Chemistry in Block Copolymer Systems of the polymerization reactor essentially “switches off” the polymerization and allows the chemist to expose the first block to air, without terminating the reactive chain end.

This technique was subsequently used to produce several types of BCP [41–45]. The thiocarbonyl end group can be removed by aminolysis or reduction with tri-nbutylstannane to leave a saturated chain end, or by thermal treatment to leave an unsaturated chain end. It may also be functionalized with amino or carboxyfunctionalized end groups [46]. 4 Atom Transfer Radical Polymerization Atom transfer radical polymerization (ATRP) is another rapidly maturing technology that easily allows the production of end-functionalized and low-polydispersity polymers.

8]; © 2006, American Institute of Physics. 4 Rod–Coil Block Copolymers There are essentially two types of BCP, both of which highlight interesting avenues for BCP self-assembly. “Coil–coil” BCPs, which are the most commonly studied, contain A and B blocks that can both be theoretically modeled as flexible chains. “Rod–coil” BCPs, on the other hand, have one polymer chain that is best represented as a rigid rod due to its stiff nature and anisotropic molecular shape. Rod-type molecules, also known as mesogens, can be incorporated into the main chain of a polymer backbone or appended from the polymer backbone as a side-chain substituent.

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